Jul 01, 2013 · Beef samples (2.0 ± 0.1 g) were minced using a coffee grinder (Model CG2B, Breville, Australia) and placed in 10 ml flat bottom headspace vials fitted with a PTFE/silicone septum and crimp cap (Supleco, USA) that contained 6% (w/w) sodium chloride. 1, 2-dichlorobenzene (2 μl, 1.3 ppm) in a 250 μl flat bottom insert was used as an internal