(Supelco, Bellefonte, PA, USA) was inserted into the headspace of a 22-ml glass vial with a polytetrafluoroethylene/silicone liner contain-ing the sample and sealed tightly with an aluminum cap (Supelco, Bellefonte, PA, USA) for sampling the volatiles. Ten different volatile compounds, including acetaldehyde, ethyl acetate, 2-methylpropanol,