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Static headspace, solid-phase microextraction and headspace 30/6/2000 · Static headspace (HS) sampling is a suitable sampling technique for determining VOCs by GC. In HS, the sample is normally placed in a sealed vial and heated in an oven until the volatile compounds reach equilibrium with the gas phase. Determination of Headspace Volatiles in Distilled Spirits Using Determination of Headspace Volatiles in Distilled Spirits Using SPME Coupled to GC. Robert E. Shirey, Michael D. Buchanan, D...

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