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GC Analysis of Terpenes in Cannabis on Equity-1 after Headspace SPME Sample Preparation fiber postbake after extraction, 3 min at 270 C Sample/Matrix 0.5 g dried cannabis in 10 mL headspace vial Desorption Process 3 min, 270 C Extraction 20 min, headspace, 40 C SPME Fiber Divinylbenzene/Carboxen Column Equity-1, 60 Automation of Sample Preparation using a GERSTEL MPS2 • Add 5 mL of sample to each 10 mL vial ( 1 minute per sample) • Prepare 5 standards + 2 AQC (30 minutes) • Add 10 µL of IS s...

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