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Determination of Headspace Volatiles in Distilled Spirits A ratio of 4 mL of sample in a 10 mL vial provided an adequate volume for the headspace to evolve, plus enough physical space for the SPME fiber to be exposed. For the fiber, a 50/30 μm divinylbenzene/Carboxen ® /polydimethylsiloxane coating on a 1 cm long StableFlex™ core was used to maximize the variety of compound types extracted. Detection of Gasoline Residues Present in Household Materials such as headspace vial heating tempera...

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